BenutzerhandbuchInhaltsverzeichnisINSTRUCTION MANUAL FOR MODEL S-4800 FIELD EMISSION SCANNING ELECTRON MICROSCOPE1FOREWORD3Scope of Instruction Manual4GUARANTEE5INSTALLATION AND AFTER-SALES SERVICE7CAUTION ON DISPOSAL OF INSTRUMENT7Available Training Programs8Handling of Chemicals8Instruction Manual8SAFETY SUMMARY9General Safety Guidelines9Electrical Hazard11High Temperature Hazard12Magnetic Field Hazard12Laser light Hazard13Warning labels on the Main unit (standard version)14Warning labels on the Display unit (standard version)15Warning labels on the Main unit (ANSI style labels)16Warning labels on the Display unit (ANSI style labels)17WARNING18Other Relevant Precautions20Emergency Off Button23Main Power Disconnect24Power Supply and Grounding Connection24INTERLOCK25Location of safety interlock26Protection from movement during earthquakes (Display unit)27Protection from movement during earthquakes (Main unit)28Gravity location of Main unit (Type1)29Gravity location of Main unit (Type2)30Gravity location of Display unit31An example of the water-leakage detector32PRECAUTIONS ON HANDLING331. PRECAUTIONS FOR TRANSPORT332. PRECAUTIONS FOR POWER CONNECTION333. GENERAL PRECAUTIONS354. MEASURES FOR EMERGENCY355. CAUTIONS ON OPERATION366. OTHERS367. FLASHING37SPECIFICATION40INSTALLATION CONDITIONS43Table of Contents461. INSTALLATION521.1 Installation Requirements521.1.1 General521.1.2 Room Temperature and Humidity521.1.3 Line Power Requirement531.1.4 Grounding531.1.5 Water Supply and Drain531.1.6 Stray Magnetic Field541.1.7 Floor Vibration551.1.8 Power Line Noise and Electric Field Noise571.1.9 Disturbance by Sound Waves581.1.10 Site requirements581.2 Materials or Instruments to be prepared by User601.3 Wiring601.3.1 Power and Ground Wirings612. FUNCTIONS632.1 Control Knobs and Switches on Main Unit642.1.1 Main unit (Column)642.2 Control Knobs and Switches on Display Unit752.2.1 Display752.3 Graphical User Interface (GUI)782.3.1 Starting the PC and logging in the S-4800 program782.3.2 S-4800 SEM Main Window802.3.3 Control arrangement on the window812.3.4 Menu832.3.5 Control Panel882.3.5.1 Functional blocks on the Control Panel882.3.5.2 HV control block882.3.5.3 Scan control block902.3.5.4 Auto control902.3.5.5 Monitoring function912.3.5.6 Magnification control912.3.5.7 Image recording922.3.5.8 Stage, Image shift control932.3.5.9 Extension for Dual screen mode942.3.6 Operation Panel952.3.6.1 SIGNAL SELECT block962.3.6.2 OPE CONDITION block972.3.6.3 R.ROTATION block982.3.6.4 SCAN MODE block982.3.6.5 SCAN SIZE block992.3.6.6 DATA ENTRY block992.3.6.7 SIGNAL PROCESSING block1002.3.6.8 TILT COMPENSATION block1012.3.6.9 COLOR MIXING block1012.3.6.10 Scroll bar and area marker block1022.3.6.11 Scroll bar and area marker block1022.3.6.12 Other optional function block1022.3.6.13 Arrangement of control blocks1032.3.7 Mouse operation on the scanning image1042.3.7.1. Exchanging mouse control functions1042.3.7.2 Focus/stigma/contrast/brightness adjustment1042.3.7.3 Stage and image shift tools1062.3.8 Setup dialog window1062.3.8.1 Column tab1072.3.8.2 Image tab1092.3.8.3 Record tab1102.3.8.4 OP. Cond tab1122.3.9 Captured Image Window1132.3.10 SEM Data Manager Window1142.3.11 Alignment Dialog Window1142.3.12 CD Measurement dialog window (option)1152.3.13 Comm Port Setting Dialog Window1152.3.14 Login Setting Dialog Window1152.3.15 Oblique Dialog Window1162.3.16 Password Setting Dialog Window1162.3.17 Save Image Dialog Window1172.3.18 Opt Signal Processing Dialog Window1172.3.19 Split/Dual Mag Controller1172.3.20 Using Short-Cut Keys1183. OPERATION1193.1 Preliminary Operation1213.1.1 Check of Column Vacuum1213.1.2 Flow the cooling water1223.1.3 Starting the Display1233.1.4 Use of Anti-Contamination Trap1243.2 Specimen Setting and Specimen Exchange1253.2.1 Cautions on Specimen Preparation1253.2.2 Specimen Preparation for Materials1253.2.3 Adjustment of Specimen Height1263.2.4 Specimen Exchange Position1263.2.5 How to Set Specimen1273.2.5.1 Extracting specimen from stage1273.2.5.2 Opening the specimen exchange chamber door1293.2.5.3 Setting a specimen1293.3 Application of High Voltage1303.3.1 Condition where the gun high voltage is applicable1303.3.2 Flashing1303.3.2.1 About flashing1303.3.2.2 Flashing Procedure1303.3.3 Setting of Accelerating Voltage and Emission Current1313.3.4 Application of High Voltage1323.4 Optimizing the Electron Beam1333.4.1 Selecting a Magnification Mode1333.4.2 Selecting Electron Optical Column Condition1333.4.2.1 High Mag mode1333.4.2.2 Low Mag Mode1373.4.3 Column Alignment Operation1383.5 Operation for Image Observation1423.5.1 SE detector1423.5.1.1 Secondary and backscattered signals and their Characteristics1433.5.1.2 Signal Control1443.5.2 Selecting Magnification1463.5.3 Selecting Scanning Speed1473.5.4 Image Brightness and Contrast Adjustment1493.5.5 Focus and Astigmatism Correction1523.5.6 Operation of the Specimen Stage (Type I - Manual Stage)1553.5.6.1 Movable range and specimen exchange position1553.5.6.2 Movable range limitation of X, Y and R axes1553.5.6.3 Tilt and Z axes limitation1563.5.6.4 3 axes motorized stage (Type1 stage option)1573.5.6.5 Stage Locking1583.5.7 Operation of the Specimen Stage (Type 2 - 5-Axis Motorized Stage)1593.5.7.1 Coordinate notation1593.5.7.2 Movable range and specimen exchange position1603.5.7.3 Setting specimen size and detectors in use1613.5.7.4 Valious operation for specimen stage1623.5.7.5 Stage tab1633.5.7.6 X, Y, R axes operation1643.5.7.7 Z and Tilt axes operation1653.5.7.8 Stage mouse operation on the scanning image1673.5.7.9 Position memory function1733.5.7.10 Stage History function1743.5.7.11 Image Navigation1753.5.7.12 Rotation Assist function1773.5.7.13 Rotation / tilt eucentric function and calibration1793.5.7.14 Stage lock1843.5.7.15 Stopping stage and Returning to previous stage position1853.5.7.16 Moveable range and limitation by optional detectors1863.6 Saving and Recording Images1893.6.1 Saving and Recording Images1893.6.2 Preparing Images for Recording1903.6.3 Setting Conditions for Image Capturing1913.6.4 Image Capturing1923.6.5 Saving a Scanning Image (Direct Save)1933.6.6 Saving Captured Images1943.6.7 Taking Photographs (Option)1943.7 Using SEM Data Manager1973.8 At the End of Daily Use1983.8.1 Turning High Voltage Off1983.8.2 Setting the Stage at the Specimen Exchange Position1983.8.3. Taking Out a Specimen1983.8.4 Closing Windows and Shutting the Display Power2003.9 Using Other Functions2013.9.1 Screen Mode2013.9.2 Split Screen and Dual Mag Mode2033.9.3 Signal Selection and Color Mixing2043.9.4 X-ray Analysis Mode2063.9.5 Signal Processing2083.9.6 Operating Condition Memory2103.9.7 Pseudo Color Display2123.9.8 Data Entry Function2123.9.9 Raster Rotation, Dynamic Focus and Tilt Compensation2153.9.11 Printing images using Report generation function2173.9.12 Copy Image2193.9.13 Copy Image information text2193.9.14 Oblique Image2203.9.15 Optional setting2213.9.16 Password Setting2233.9.17 Setting Login Name2233.10 Image Quality2253.10.1 Accelerating Voltage and Image Quality2253.10.2 Condenser Lens Setting and Image Quality2263.10.3 Objective Lens Aperture Size and Image Quality2263.11 Mechanical Column Alignment2273.11.1 Preparative Operation for Alignment2273.11.2 Mechanical Alignment of the Electron Gun2283.11.3 Alignment of the Beam Monitor Aperture2283.11.4 Alignment of the Objective Lens Aperture2293.11.5 Mechanical Alignment of the First Condenser Lens2293.11.6 Mechanical Alignment of the Second Condenser Lens2293.11.7 Stigma Alignment (electro-magnetic alignment)2303.11.8 Aperture Alignment (electro-magnetic alignment)2303.12 Using SEM Data Manager2323.12.1 Precaution About SEM Data Manager2323.12.2 Functions2333.12.2.1 Image Database2333.12.2.2 Menu and tool buttons2343.12.3 Operation2373.12.3.1 Registering Images on SEM Data Manager Database2373.12.3.2 Selecting User name and opening data tree2383.12.3.3 Image display2393.12.3.4 Image information2403.12.3.5 Viewer display2403.12.3.6 Data Entry2403.12.3.7 Contrast Conversion2433.12.3.8 Image Processing2463.12.3.9 Color Mixing2473.12.3.10 Printing images2493.12.3.11 Image file operation2493.12.3.12 Batch operation of image files2503.12.3.13 Slide show2523.12.3.14 Optimizing and repairing database file2524. MAINTENANCE2534.1 Maintenance of Electron optical Column2534.1.1 Maintaining Vacuum of Electron Gun and Intermediate Chamber2534.1.2 Replacement and Cleaning of Objective Lens Aperture2534.1.3 Cleaning of Aperture Plates2554.2 Maintenance of Rotary Pump (Only for P/N 539-9010 and 539-9060)2574.2.1 Oil Change2574.2.2 Replacement of Oil Mist Trap2584.2.3 Troubleshooting2594.3 Maintenance of Air Compressor(Only for P/N 539-9010 and 539-9060)2604.3.1 Checkup and Maintenance2604.3.2 Troubleshooting of Air Compressor2624.3.3 Location and Functions of Major Components2634.4 Troubleshooting2644.4.1 When Column Evacuation does not Work2644.4.2 When Specimen Exchange Chamber Vacuum is not Good2644.4.3 When Specimen Chamber Vacuum is not Good2654.4.4 When Ion Pump Vacuum Degraded2654.4.5 When Emission Current is not Set at Normal Value2664.4.6 When Image is not Shown on Screen2664.4.7 When Image is Very Noisy2674.4.8 When You cannot Correct Astigmatism2684.4.9 When Auto Focus or Auto Stigma does not Work Satisfactorily2684.4.10 When S-4800 control program does not start up2694.4.11 When PC has Hanged up2694.4.12 When Error Messages are shown2704.5 Operation for shutting down all power supply of S-48002704.6 Operation when power was shut down by power line failure2704.7 Operation for Starting S-48002714.8 Operation when power line failure recovered2724.9 Operation when Water supply stopped by failure2724.10 Gun Baking operation2734.11 Caution on Maintenance2775. REPLACEMENT PARTS2785.1 Consumables and Spare Parts2785.1.1 Consumables2785.1.2 Replacement Parts2795.1.3 Spare Parts2806. ACCESSORY OPERATION2816.1 Model S-5080 Auto-Camera (option)2816.1.1 Configuration2816.1.2 Specifications2836.1.3 Assembling the Camera2856.1.4 Operation2866.2 Installation Manual for the SEC Guide Rail (for Installer)287INDEX288Größe: 6,94 MBSeiten: 294Language: EnglishHandbuch öffnen