Teledyne T201 Manuel D’Utilisation

Page de 44
Teledyne API Model T201 NH
Analyzer Operator Manual
 
Calibration Procedure
 
07271B DCN6646 
19 
Table 2-4. NO Calibration Procedure - NO Gas through the SPAN Port 
Step No. 
Action 
Comment 
1. Press 
CALS 
The T201 enters the calibrate mode from sample 
mode. The NO gas is supplied through the SPAN inlet 
port on the rear panel of the M501 NH
3
Table 2.3 
 
Notes 
  Both the TN
x
 and NO
x
 channels must be spanned individually with nitric 
oxide gas. When you span the NO
x
 channel both the NO and NO
x
 
concentrations must be manually inputted.  
  It is recommended that the calibration of both the TN
x
 and NO
x
 
channels be done at the same time.  
  Always confirm that SPAN gas is flowing past the sample or span port 
on the rear of the M501 NH
3
 converter. There should always be some 
excess flow. If insufficient flow is supplied to the analyzer ambient gas 
will be entrained and the span values will be incorrect. However, it is 
important not to over pressurize the analyzer.  
  It is a good idea to allow the analyzer to sample span gas for extended 
periods following span calibration. Large drifts can signify leaks or 
indicate an issue with the span gas source.  
  If after spanning with nitric oxide, the analyzer slopes are out of range 
conduct the following: 
 - Confirm the gas sources are good. Usually the bottle is certified to a 
known level of nitric oxide. The bottle should be balanced with nitrogen.  
- Try not to use the same regulator for nitric oxide as was used on 
ammonia. This also holds for the tubing between the different bottles 
and the mixing source (calibrator). 
 - Confirm the zero reading is good by delivering Zero gas. 
 - Confirm that the concentration delivered to the analyzer is equal to 
what you entered under the 
CONC menu NOx and TNx. 
 - Leak check both the M501 NH
3
 and analyzer together. 
 - Using section 11.6.5 of the T200 manual confirm that the PMT sensor 
hardware calibration is set correctly. 
2.3  S
PANNING THE 
A
NALYZER WITH 
A
MMONIA 
G
AS