Teledyne t320u Manuale Utente

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Calibration Procedures 
Teledyne API – Model T300/T300M CO Analyzer 
198 
9.1.1.1. ZERO AIR 
Zero air or zero calibration gas is defined as a gas that is similar in chemical 
composition to the measured medium but without the gas to be measured by the 
analyzer. 
For the T300/T300M zero air should contain less than 25 ppb of CO and other major 
interfering gases such as CO and Water Vapor.  It should have a dew point of -5
C or 
less. 
If your application is not a measurement in ambient air, the zero calibration gas should 
be matched to the composition of the gas being measured.   
  Pure nitrogen (N
2
) can be used as a zero gas for applications where CO is 
measured in nitrogen. 
  If your analyzer is equipped with an external zero air scrubber option, it is capable of 
creating zero air from ambient air.   
For analyzers without the zero air scrubber, a zero air generator such as the Teledyne 
API’s T701 can be used.  Please visit the company website for more information. 
9.1.1.2. SPAN GAS 
Span Gas is a gas specifically mixed to match the chemical composition of the type of 
gas being measured at near full scale of the desired measurement range.  It is 
recommended that the span gas used have a concentration equal to 80-90% of the full 
measurement range.   
If Span Gas is sourced directly from a calibrated, pressurized tank, the gas mixture 
should be CO mixed with Zero Air or N
2
 at the required ratio. 
For oxygen measurements using the optional O
2
 sensor, we recommend a reference gas 
of 21% O
2
 in N
2
.   
  For quick checks, ambient air can be used at an assumed concentration of 20.8%.   
 Generally, 
O
2
 concentration in dry, ambient air varies by less than 1%. 
9.1.1.3. CALIBRATION GAS STANDARDS AND TRACEABILITY 
All equipment used to produce calibration gases should be verified against standards of 
the National Institute for Standards and Technology (NIST).  To ensure NIST 
traceability, we recommend to acquire cylinders of working gas that are certified to be 
traceable to NIST Standard Reference Materials (SRM).  These are available from a 
variety of commercial sources. 
Table 9-1: 
NIST-SRMs Available for Traceability of CO Calibration Gases 
NIST-SRM Type  Nominal 
Concentration 
680b 
CO in N
2
 500 
ppm 
1681b 
CO in N
2
 1000 
ppm 
2613a 
CO in Zero Air 
20 ppm 
2614a 
CO in Zero Air 
45 ppm 
2659a1 O
2
 in N
2
 
21% by weight 
2626a CO
2
 in N
2
 
4% by weight 
27452 CO
2
 in N
2
 
16% by weight 
1
 Used to calibrate optional O
 sensor. 
2
 Used to calibrate optional CO
2
 sensor. 
 
Note 
It is generally a good idea to use 80% of the reporting range for that channel for 
the span point calibration. 
For instance, if the reporting range of the instrument is set for 50.0 PPM, the 
proper span gas would be 40.0 PPM.
 
06864B DCN6314