Teledyne t320u Manuale Utente

Pagina di 426
Teledyne API – Model T300/T300M CO Analyzer 
EPA Calibration Protocol 
233 
Table 10-1:  Matrix for Calibration Equipment & Supplies 
EQUIPMENT & 
SUPPLIES 
SPECIFICATION 
REFERENCE 
ACTION IF 
REQUIREMENTS ARE NOT
MET 
Recorder 
Compatible with output 
signal of analyzer; min. 
chart width of 150 mm (6 in) 
is recommended 
 
Return equipment to supplier
Sample line and 
manifold 
Constructed of PTFE or 
glass 
Check upon receipt 
Return equipment to supplier
Calibration equipment 
Q.A. Handbook
1
 Vol II Part 1 , App 15,  
Sec. 4.4 & 5.4 
Return equipment/ supplies 
to supplier or take corrective 
action 
Detection limit 
Noise = 0.5 ppm 
Lower detectable 
limit=1.0 ppm 
40 CFR, Pt 53.20 & 23
Instruments designated as 
reference or equivalent have 
been determined to meet 
these acceptance criteria. 
Working standard CO 
cylinder gas 
Traceable to NIST-SRM 
Analyzed against NIST-SRM;
40 CFR, Pt 50, App C; para.  
3.1
Obtain new working 
standard and check for 
traceability 
Zero air 
Clean dry ambient air, free 
of contaminants that cause 
detectable response with 
the CO analyzer. 
40 CFR, Pt 50, App C; para.  
3.2
Obtain air from another 
source or regenerate. 
Record form 
Q.A. Handbook
1
 Vol II Part 1 , App 15,  
Table A-5 & A-6 
Revise forms as appropriate
Audit equipment 
Must not be the same as 
used for calibration 
Q.A. Handbook
1
Vol II Part 1 , 
App 15,  
Sec. 4.4 & 5.4 
Locate problem and correct 
or return to supplier 
 
10.1.3. RECOMMENDED STANDARDS FOR ESTABLISHING TRACEABILITY 
To assure data of desired quality, two considerations are essential:  
  The measurement process must be in statistical control at the time of the 
measurement. 
  The systematic errors, when combined with the random variation in the 
measurement process, must result in a suitably small uncertainty. 
Evidence of good quality data includes documentation of the quality control checks and 
the independent audits of the measurement process by recording data on specific forms 
or on a quality control chart and by using materials, instruments, and measurement 
procedures that can be traced to appropriate standards of reference.  
To establish traceability, data must be obtained routinely by repeat measurements of 
standard reference samples (primary, secondary and/or working standards).  More 
specifically, working calibration standards must be traceable to standards of higher 
accuracy, such as those listed in Table 3-12. 
Cylinders of working gas traceable to NIST-SRMs (called EPA Protocol Calibration 
Gas) are also commercially available (from sources such as Scott Specialty Gases, etc.).  
See Table 3-12 for a list of appropriate SRMs. 
06864B DCN6314