用户手册目录ICS-2100 Ion Chromatography System Operator’s Manual1Contents31 . Introduction131.1 Introduction to Ion Chromatography (IC)131.2 Overview of the ICS-2100161.3 About This Manual171.3.1 Safety Messages and Notes181.4 Safety and Regulatory Information201.4.1 Safety Labels202 . Features232.1 Operating Features232.1.1 Front Panel232.1.2 Top Cover282.1.3 Component Panel302.1.4 Rear Panel332.2 Flow Schematics352.3 Chromeleon and Chromeleon Xpress422.3.1 The Panel Tabset422.3.2 Software Control Modes432.3.3 System Wellness432.4 System Component Details442.4.1 Vacuum Degas Assembly (Optional)442.4.2 Eluent Valve462.4.3 Pump462.4.4 Eluent Generator492.4.5 Auxiliary Power Supply (Optional)542.4.6 Injection Valve542.4.7 Auxiliary Valve (Optional)562.4.8 Column Heater572.4.9 Suppressor582.4.10 DS6 Heated Conductivity Cell583 . Operation and Maintenance613.1 Operation Overview613.2 Turning On the System Power633.3 Connecting to Chromeleon643.4 Set Up the Eluent Reservoir663.4.1 Filter the Deionized Water663.4.2 Fill the Reservoir663.4.3 Set the Eluent Level663.4.4 Connect the Reservoir683.5 Check All Connections693.6 Prime the Pump693.7 Set System Operating Conditions703.8 Equilibrate the System and Verify Operational Status713.9 Prepare Samples723.9.1 Collecting and Storing Samples723.9.2 Pretreating Samples733.9.3 Diluting Samples733.10 Loading and Injecting Samples743.10.1 Loading Samples with a Syringe753.10.2 Loading Samples with a Vacuum Syringe763.10.3 Loading Samples with an Autosampler763.10.4 Injecting Samples773.11 Processing Samples773.11.1 Manual Sample Processing773.11.2 Automatic (Batch) Sample Processing783.12 Maintenance804 . Troubleshooting834.1 Error Messages834.2 Troubleshooting Error Messages864.3 Liquid Leaks984.4 Pump Difficult to Prime or Loses Prime1004.5 Pump Does Not Start1024.6 No Flow1024.7 Erratic Flow/Pressure Reading1034.8 Excessive System Backpressure1044.9 Peak “Ghosting”1054.10 Nonreproducible Peak Height or Retention Time1064.11 Abnormal Retention Time or Selectivity1064.12 No Cell Response1064.13 High Cell Output1074.14 Baseline Noise or Drift1084.15 Vacuum Degas Assembly Does Not Run1095 . Service1115.1 Diagnostic and Calibration Procedures1115.1.1 Chromeleon Wellness Panel Overview1125.1.2 Diagnostic and Calibration Touch Screen Overview1145.1.3 Calibrating the Conductivity Cell1155.1.4 Calibrating the Flow Rate1185.1.5 Calibrating the Vacuum Degas Assembly1205.2 Isolating a Restriction in the Liquid Lines1215.3 Replacing Tubing and Fittings1255.4 Rebuilding the Injection Valve or Auxiliary Valve1265.5 Replacing an Auxiliary Valve Pod1285.6 Cleaning and Replacing the Pump Check Valves1305.7 Replacing a Pump Piston Seal and Piston Rinse Seal1325.8 Replacing a Pump Piston1365.9 Replacing the Waste Valve or Priming Valve O-Ring1375.10 Replacing the Conductivity Cell1395.11 Replacing the Suppressor1425.12 Replacing the Column Heater1435.13 Replacing the Column Heater Heat Exchanger1465.14 Replacing the Eluent Valve1475.15 Replacing the Leak Sensor1495.16 Priming the Pump1505.16.1 Priming the Eluent Lines with a Syringe1505.16.2 Priming with the Prime Button1525.17 Priming the Pump with Isopropyl Alcohol1535.18 Changing Main Power Fuses1545.19 Replacing an EluGen Cartridge1555.19.1 Replacing a KOH, LiOH, MSA, or NaOH EluGen Cartridge1555.19.2 Replacing a K2CO3 Cartridge1635.20 Replacing the CR-TC1775.21 Replacing the EPM Electrolytic pH Modifier1815.21.1 Recording the EPM Serial Number in Chromeleon1825.21.2 Plumbing the EPM for Hydrating and Conditioning1835.21.3 Hydrating and Conditioning the EPM1855.22 Replacing the EGC CO3 Mixer1865.22.1 Installing the New EGC CO3 Mixer1865.22.2 Filling the EGC CO3 Mixer with Deionized Water1875.22.3 Filling the EGC CO3 Mixer with Eluent1905.23 Replacing the EGC Holder and Degas Assembly1975.23.1 Disconnecting and Removing the EluGen Cartridge1975.23.2 Removing the CR-TC and Reinstalling it in the New EGC Holder2005.23.3 Removing the EPM and Reinstalling it in the New EGC Holder2025.23.4 Installing the New EGC Holder Without a CR-TC or EPM2045.23.5 Reinstalling the EluGen Cartridge205A . Specifications207A.1 Electrical207A.2 Physical207A.3 Environmental208A.4 Front Panel208A.5 Analytical Pump and Fluidics208A.6 Eluent Generation210A.7 Detector Electronics212A.8 Conductivity Cell with Heat Exchanger212A.9 Injection Valve214A.10 Auxiliary Valve (Optional)214A.11 Vacuum Degas Assembly214A.12 Column Heater214A.13 Auxiliary Power Supply (Optional)214A.14 Suppressors215A.15 Autosampler216A.16 System Software216B . Touch Screen Operation219B.1 Using the Touch Screen219B.2 Using the Touch Screen with Chromeleon222B.3 Overview of ICS-2100 Touch Screen Pages223B.4 Home Page224B.4.1 Home Page Pump Controls224B.4.2 Home Page EGC Controls226B.4.3 Home Page Column Heater226B.4.4 Home Page Injection Valve Controls227B.4.5 Home Page Detector Controls227B.4.6 Other Home Page Controls228B.5 Plot Page229B.6 Status Page230B.6.1 Viewing Other Status Parameters232B.6.2 Status Parameter Details233B.7 Pump Page235B.7.1 Setting Pump Pressure Limits and Selecting the Pressure Unit235B.7.2 Setting Degas Operating Parameters (Optional)236B.7.3 Controlling the Eluent Valve237B.8 Eluent Generator Page238B.8.1 EGC Serial Number238B.8.2 Setting the Eluent Concentration239B.8.3 Controlling the Eluent Generator Power240B.8.4 Monitoring the EluGen Cartridge Life240B.8.5 Controlling the CR-TC Power241B.9 Suppressor Page242B.10 Detector Page243B.10.1 Setting the Data Rise Time244B.10.2 Selecting the Conductivity Polarity244B.10.3 Setting Analog Out Options245B.11 Information Page246B.12 Module Setup Page247B.13 Input/Output Page248B.14 Diagnostic and Calibration Pages248C . TTL and Relay Control251C.1 TTL and Relay Connections251C.1.1 Selecting TTL Input Functions and Control Types254C.2 Controlling TTL and Relay Outputs257C.3 Example Setup for Stand-Alone Operation258D . Reordering Information263E . FAQ267E.1 How do I hook up an autosampler?267E.2 How do I print?267E.3 Why are the retention times moving?267E.4 How do I adjust retention times?267E.5 When should I remake standards?267E.6 When should I replace the eluent generator cartridge?268E.7 How do I start Chromeleon?268E.8 How do I delete data?268E.9 How do I back up data?268E.10 How do I shut off the system?268E.11 How do I store columns?268E.12 How do I know when a column is dirty?269E.13 How do I clean a column?269E.14 Why is the conductivity high?269E.15 How do I configure and operate the auxiliary valve?269F . Glossary271Index277文件大小： 4.1 MB页数： 288Language: English打开用户手册
